1664, by Robert Boyle. Read the full text.
Boyle's 'Experiments and considerations touching colours'
Michael Robinson • Link
Boyle, Robert, 1627-1691.
Experiments and considerations touching colours. First occasionally written, among some other essays, to a friend; and now suffer’d to come abroad as the beginning of an experimental history of colours. By the Honourable Robert Boyle, Fellow of the Royal Society.
[Variant title: Short account of some observations made by Mr. Boyle about a diamond that shines in the dark ]
London : printed for Henry Herringman at the Anchor in the lower walk of the New-Exchange, MDCLXIV. 
8vo., , 423,  p., folded plate. Title page printed in red and black. "A short account of some observations made by Mr. Boyle about a diamond that shines in the dark" has separate dated title page; pagination and register are continuous.
Wing (2nd ed., 1994), B3967; Fulton, J. Boyle, # 57
Published in Latin the following year:
Experimenta et considerationes de coloribus, primùm ex occasione, inter alias quasdam diatribas, ad amicum scripta, nunc verò in lucem prodire passa, ceu initium historiæ experimentalis de coloribus. A Roberto Boyle nobilie anglo, et Societatis Regiæ membro.
Londini : impensis Henrici Herringman, MDCLXV. 
12mo., , 444 p. Title page prited in red and black; initial imprimatur leaf. "Brevis Enarratio quarundam observationum" has a separate title page dated 1664 on leaf T1r.
Wing (2nd ed., 1994), B3958; Fulton, J. Boyle, #59
English text reprinted 1670.
San Diego Sarah • Link
It appears Pepys read this in Latin. The above says the English version was printed in 1670.
Chart showing the number of references in each month of the diary’s entries.
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